LIBS Info: Element Analysis
Title | Authors | Material | Detector | Spectrometer | Software |
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New near-infrared LIBS detection technique for sulfur | George Asimellis, A. Giannoudakos, M. Kompitsas | Sulphur | Andor iStar III | Jobin-Yvon HRP | |
Laser: | Nd:YAG 355.0000nm 26.0000mJ 5.000Hz |
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Gate Delay: | 1.000us | ||||
Gate Width: | 5.000us | ||||
Analysis is made of S powder in Ca(NO3)2 pressed into pellets. However, the main point of the paper is to explore the detection limits for S. |
Element | Detection Limit (ppm) | Wavelength (nm) | Other Wavelengths (nm) | Calibration Method | Calibration Range (ppm) | Notes |
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S | 5000.0000 (Minimum concentration detected) | 869.4600 | N/A | Univariate Calibration | 5000.0000-200000.0000 | The 869.46nm peak was chosen as their detector did not have good sensitivity and the stronger 921.28/922.81/92..75nm triplet. Data collected under He atmosphere. Signal strength dependent on He pressure, with best results at 100-200mbar. No ratioing was performed, as there were no suitable peaks in the available spectrum around the S peak at 869.46nm. |
Element | RMSE (ppm) | Wavelength (nm) | Calibration Method | Notes |
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