LIBS Info: Element Analysis
| Title | Authors | Material | Detector | Spectrometer | Software |
|---|---|---|---|---|---|
| Detection of bromine in thermoplasts from consumer electronics by laser-induced plasma spectroscopy | I. Radivojevic, R. Niessner, C. Haisch, S. Florek, H. Becker-Ross, U. Panne | Plastic | Electron Tubes Inc 9635B | Acton VM 504 | |
| Laser: | Nd:YAG 1064.0000nm 430.0000mJ 10.000Hz |
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| Gate Delay: | Noneus | ||||
| Gate Width: | Noneus | ||||
| Detection limits in the VUV and the UV/Vis/IR are compared in this paper. The UV/Vis/IR results are described here. Only a Photomultiplier was used here, with the spectrum built up by stepping the monochromator. | |||||
| Element | Detection Limit (ppm) | Wavelength (nm) | Other Wavelengths (nm) | Calibration Method | Calibration Range (ppm) | Notes |
|---|---|---|---|---|---|---|
| Br | 500.0000 (Stated) | 130.9900 | 148.85nm, 153.17nm, 157.48nm, 163.34nm, 131.67/131.74/131.77nm | Univariate Calibration | -10.0000--10.0000 | Experiments were performed in both 2l/min Ar flow and a static atmosphere of 1000mbar. Under the gas flow several peaks were detected which were apparent in the static atmosphere. The build up of molecular oxygen in the chamber was thought to be the cause of the difference. Ratioing the 130.99 Br I peak to C I at 193.09nm improved the performance. |
| Element | RMSE (ppm) | Wavelength (nm) | Calibration Method | Notes |
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