LIBS Info: Element Analysis

Title	Authors	Material	Detector	Spectrometer	Software
Determination of Impurities in Uranium and Plutonium Dioxides by Laser-Induced Breakdown Spectroscopy	Christophe Moulin, Patrick Mauchien, Pascal Fichet	Nuclear	Princeton Instruments ICCD Max	Jobin Yvon HR1000	Winspec
Laser:	Nd:YAG 532.0000nm 15.0000mJ 10.000Hz
Gate Delay:	3.000us
Gate Width:	5.000us
The authors characterised the detection limits for key impurities in Plutonium and Uranium Oxides pellets. Spectra of a limited wavelength range around the nominated peak for each element were collected. Detection limits are estimates based on comparison of blank and spectra of a known concentration.

LOD
RMSEP

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Element	Detection Limit (ppm)	Wavelength (nm)	Other Wavelengths (nm)	Calibration Method	Calibration Range (ppm)	Notes
Ag	60.0000 (Estimation)	328.0683	N/A	None	0.0000-116.0000	Estimated by comparison of Blank and Max concentration spectra.
Ag	200.0000 (Estimation)	328.0683	N/A	None	0.0000-538.0000	Estimated by comparison of Blank and Max concentration spectra.
Al	200.0000 (Estimation)	396.1527	N/A	None	0.0000-382.0000	Estimated by comparison of Blank and Max concentration spectra.
B	65.0000 (Estimation)	249.7733	N/A	None	0.0000-487.0000	Estimated by comparison of Blank and Max concentration spectra.
Ba	100.0000 (Estimation)	455.4042	N/A	None	0.0000-399.0000	Estimated by comparison of Blank and Max concentration spectra.
Ba	600.0000 (Estimation)	455.4040	N/A	None	0.0000-703.0000	Estimated by comparison of Blank and Max concentration spectra.
Bi	350.0000 (Estimation)	306.7716	N/A	None	0.0000-795.0000	Estimated by comparison of Blank and Max concentration spectra.
Cr	35.0000 (Estimation)	520.8436	N/A	None	0.0000-76.0000	Estimated by comparison of Blank and Max concentration spectra.
Cr	70.0000 (Estimation)	520.8436	N/A	None	0.0000-510.0000	Estimated by comparison of Blank and Max concentration spectra.
Cu	90.0000 (Estimation)	324.7540	N/A	None	0.0000-91.0000	Estimated by comparison of Blank and Max concentration spectra.

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Element	RMSE (ppm)	Wavelength (nm)	Calibration Method	Notes
No data available in table

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