LIBS Info: Element Analysis
Title | Authors | Material | Detector | Spectrometer | Software |
---|---|---|---|---|---|
Critical evaluation of gated CCD detectors for laser-induced breakdown spectroscopy analysis | M. Sabsabi, R. Heon, L. St-Onge | Copper Alloy | Ocean Optics HR2000 | Ocean Optics HR2000 | |
Laser: | Nd:YAG 1064.0000nm 60.0000mJ 2.000Hz |
||||
Gate Delay: | 2.000us | ||||
Gate Width: | Noneus | ||||
Paper compares the performance of an ICCD and Ocean Optics spectrometer/detection system. ICCD results are here for aluminium alloys, here for copper alloys , Ocean Optic are at here for aluminium alloys and here for copper alloys. Experiments were performed under common conditions, and then conditions optimised for each detector The authors note that their Ocean Optics spectrometer had a 250ns timing jitter that has been fixed on subsequent models |
Element | Detection Limit (ppm) | Wavelength (nm) | Other Wavelengths (nm) | Calibration Method | Calibration Range (ppm) | Notes |
---|---|---|---|---|---|---|
Ni | 650.4000 (Stated) | 341.4800 | 305.08 | Univariate Calibration | -10.0000--10.0000 | LODs range from 851-1702ppm, depending on conditions |
Ag | 110.8000 (Stated) | 328.0700 | N/A | Univariate Calibration | -10.0000--10.0000 | LODs range: 110.8-221.6ppm |
Fe | 1230.7000 (Stated) | 372.0000 | N/A | Univariate Calibration | -10.0000--10.0000 | LODs range: 1230.7-2461.5ppm |
Element | RMSE (ppm) | Wavelength (nm) | Calibration Method | Notes |
---|