LIBS Info: Element Analysis
| Title | Authors | Material | Detector | Spectrometer | Software |
|---|---|---|---|---|---|
| Exploring laser-induced breakdown spectroscopy for nuclear materials analysis and in-situ applications | Nicolas Andre, Rodger C. Martin, Deanne J. Brice, Steve Allman, Madhavi Z. Martin | Liquids | Andor ICCD | Czerny-Turner (Unspecified) | Solis |
| Laser: | Nd:YAG 532.0000nm 50.0000mJ 10.000Hz |
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| Gate Delay: | Noneus | ||||
| Gate Width: | Noneus | ||||
| Liquids for analysis were dried onto pellets of CaCO3 and Graphite. In general, the graphite pellets yielded lower detection limits. | |||||
| Element | Detection Limit (ppm) | Wavelength (nm) | Other Wavelengths (nm) | Calibration Method | Calibration Range (ppm) | Notes |
|---|---|---|---|---|---|---|
| Cs | 600.0000 (Smallest Peak Observed) | 852.1000 | N/A | Univariate | 600.0000-10000.0000 | No LIBS peaks were detected for Cs on CaCO3 pellets, but detection limit of 600pm observed on the graphite pellet |
| Ce | 100.0000 (Smallest Peak Observed) | 305.8000 | 303 | Univariate | 100.0000-10000.0000 | Significantly better detection limits for analysis of liquid dried onto graphite pellets compared to CaCO3. Authors attribute this to better laser absorption leading to more energy transmitted into the plasma |
| Sr | 10.0000 (Smallest Peak Observed) | None | N/A | Univariate | 10.0000-1000.0000 | Not the main focus of this paper. Obtained by drying solution onto CaCO3 pellet |
| Element | RMSE (ppm) | Wavelength (nm) | Calibration Method | Notes |
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