LIBS Info: Element Analysis
Title | Authors | Material | Detector | Spectrometer | Software |
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Elemental profiling and determination of Ti content of the beach sand samples of Bangladesh using LIBS technique | A.F.M.Y Haider, M. Wahadoszamen, M.E. Sadat, K.M. Abedin, A.I. Talukder | Geological | Acton Spectra Pro | Acton Spectra Pro | |
Laser: | Nd:YAG 532.0000nm 450.0000mJ 10.000Hz |
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Gate Delay: | Noneus | ||||
Gate Width: | Noneus | ||||
In this work, beach sand samples were washed with distilled water, dried, powdered (using hand mortar) then pressed into a pellet for analysis. A range of some 20 elements were identified, but the Ti concentration only was quantified. Quantification in an unknown sample involved the construction of calibration curves using standard additions for 6 different Ti peaks . A non-gated, non-intensified CCD was used for this analysis. |
Element | Detection Limit (ppm) | Wavelength (nm) | Other Wavelengths (nm) | Calibration Method | Calibration Range (ppm) | Notes |
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Ti | 2000.0000 (Calibration Curve Slope) | -10.0000 | 489.991, 498.1732, 499.107, 499.951, 503.591, 506.466 | Univariate Calibration | -10.0000--10.0000 | Analysis involved standard additions of TiO and determining the unknown concentration using 6 Ti peaks [489.991nm, 498.1732nm, 499.107nm, 499.9504nm, 503.587nm, 506.48nm] ratioed to a nearby Fe Peak [495.7597nm] |
Element | RMSE (ppm) | Wavelength (nm) | Calibration Method | Notes |
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